Pentafluoropyridine as a fluorinating reagent for preparing a hydrocarbon soluble beta-diketiminatolead(II) monofluoride
2011 | journal article. A publication with affiliation to the University of Göttingen.
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Pentafluoropyridine as a fluorinating reagent for preparing a hydrocarbon soluble beta-diketiminatolead(II) monofluoride
Jana, A.; Sarish, S. P.; Roesky, H. W.; Leusser, D.; Objartel, I. & Stalke, D. (2011)
Chemical Communications, 47(19) pp. 5434-5436. DOI: https://doi.org/10.1039/c1cc11310k
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Details
- Authors
- Jana, Anukul; Sarish, Sankaranarayana Pillai; Roesky, Herbert W.; Leusser, Dirk; Objartel, Ina; Stalke, Dietmar
- Abstract
- A well-designed method for the preparation of a beta-diketiminato lead(II) monofluoride has been developed using LPbNMe(2) (L = [CH{C(Me)(2,6-iPr(2)C(6)H(3)N)}(2)]) and pentafluoropyridine (C(5)F(5)N). The resulting LPbF was used for the synthesis of amidinatosilicon(II) monofluoride. Moreover the activation of a ketone was observed when the LPbF was treated with PhCOCF(3).
- Issue Date
- 2011
- Status
- published
- Publisher
- Royal Soc Chemistry
- Journal
- Chemical Communications
- ISSN
- 1359-7345
- Sponsor
- Deutsche Forschungsgemeinschaft; DNRF