Acetylacetonatodifluorooxometalates of vanadium and molybdenum: syntheses and crystal structures

2001 | journal article. A publication with affiliation to the University of Göttingen.

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​Acetylacetonatodifluorooxometalates of vanadium and molybdenum: syntheses and crystal structures​
Stasch, A. ; Schormann, M.; Prust, J.; Roesky, H. W. ; Schmidt, H. G. & Noltemeyer, M.​ (2001) 
Dalton Transactions,(13) pp. 1945​-1947​.​ DOI: https://doi.org/10.1039/b100740h 

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Authors
Stasch, A. ; Schormann, M.; Prust, J.; Roesky, H. W. ; Schmidt, H. G.; Noltemeyer, M.
Abstract
[Et4N][HF2] reacted with VO(acac)(2) and MoO2(acac)(2) in acetonitrile at room temperature with elimination of Hacac to produce the metalates [Et4N][(acac)VOF2] 1 and [Et4N][(acac)MoO2F2] 2, respectively. These compounds are the first examples of fluorometalates of vanadium and molybdenum bearing the acetylacetonato group. The crystal structures have been determined.
Issue Date
2001
Status
published
Publisher
Royal Soc Chemistry
Journal
Dalton Transactions 
ISSN
1472-7773

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