Synthesis and Characterization of Heterobimetallic Aluminum-Germanium(IV) Disulfides
2008 | journal article. A publication with affiliation to the University of Göttingen.
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Synthesis and Characterization of Heterobimetallic Aluminum-Germanium(IV) Disulfides
Yang, Z.; Ma, X.; Zhang, Z.; Roesky, H. W.; Magull, J. & Ringe, A. (2008)
Zeitschrift für anorganische und allgemeine Chemie, 634(15) pp. 2740-2742. DOI: https://doi.org/10.1002/zaac.200800030
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Details
- Authors
- Yang, Zhi; Ma, Xiaoli; Zhang, Z.; Roesky, Herbert W.; Magull, Joerg; Ringe, Arne
- Abstract
- Three heterobimetallic aluminum-germanium(IV) disulfides are synthesized. The reaction of {LAl[(SLi)(2)(THF)(2)]}(2) (1) (L = HC(CMeNAr)(2), Ar = 2,6-iPr(2)C(6)H(3)) with Ph(2)GeCl(2), Me(2)GeCl(2), and GeCl(4). respectively, in THF afforded LA1(mu-S)(2)GePh(2) (2), LA1(mu-S)(2)GeMe(2) (3) and LA1(mu-S)(2)Ge(mu-S)(2)AIL (4) in good yields. Compounds 2, 3 and 4 were investigated by elemental analysis, NMR, EI-MS and 3 was also characterized by single crystal X-ray structural analysis.
- Issue Date
- 2008
- Status
- published
- Publisher
- Wiley-v C H Verlag Gmbh
- Journal
- Zeitschrift für anorganische und allgemeine Chemie
- ISSN
- 0044-2313
- Sponsor
- Fonds der Chemischen Industrie; Gottinger Akademie der Wissenschaften
