Low-cost conversion of a coaxial nozzle arrangement into a stationary low-temperature attachment

1996 | journal article. A publication with affiliation to the University of Göttingen.

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​Low-cost conversion of a coaxial nozzle arrangement into a stationary low-temperature attachment​
Kottke, T.; Lagow, R. J. & Stalke, D.​ (1996) 
Journal of Applied Crystallography29(4) pp. 465​-468​.​ DOI: https://doi.org/10.1107/S0021889896003172 

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Authors
Kottke, Thomas; Lagow, Richard J.; Stalke, Dietmar
Abstract
A stationary nozzle accessory designed for the Siemens/Nicolet LTII low-temperature device with standard [varphi]-coaxial nozzle arrangement is described. The attachment is easy to assemble and its compatibility allows interchanging between both systems in less than 1 h, if required. Implementation of the stationary nozzle reduces the consumption of liquid nitrogen by more than 40% and extends the temperature range available for data collection by 60 K in the lower temperature range. Details of construction are presented, and a comparison with the [varphi]-coaxial nozzle is discussed.
Issue Date
1996
Journal
Journal of Applied Crystallography 
Organization
Fakultät für Chemie 
File Format
application/pdf
Language
English

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