Fakultät für Chemie

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  • 1999 | Journal Article | 
    ​ ​Advances in direct methods for protein crystallography​
    Usón, I. & Sheldrick, G. M.​ (1999) 
    Current Opinion in Structural Biology, 9(5) pp. 643​-648​.​ DOI: https://doi.org/10.1016/S0959-440X(99)00020-2 
    ​Details  DOI 
  • 1996 | Journal Article | 
    ​ ​TAPSO at low temperature​
    Wouters, J. & Stalke, D.​ (1996) 
    Acta Crystallographica / C, 52(7) pp. 1684​-1686​.​ DOI: https://doi.org/10.1107/S0108270196001199 
    ​Details  DOI 
  • 1996 | Journal Article | 
    ​ ​Low-cost conversion of a coaxial nozzle arrangement into a stationary low-temperature attachment​
    Kottke, T.; Lagow, R. J. & Stalke, D.​ (1996) 
    Journal of Applied Crystallography, 29(4) pp. 465​-468​.​ DOI: https://doi.org/10.1107/S0021889896003172 
    ​Details  DOI 
  • 1994 | Journal Article | 
    ​ ​Lanthanide alkoxides—III. Four-coordinate anionic neodymium(III) alkoxides and amides 1​
    Edelmann, F. T.; Steiner, A.; Stalke, D.; Gilje, J. W.; Jagner, S. & Håkanssons, M.​ (1994) 
    Polyhedron, 13(4) pp. 539​-546​.​ DOI: https://doi.org/10.1016/S0277-5387(00)84729-4 
    ​Details  DOI 
  • 1994 | Journal Article | 
    ​ ​Structure and crystal packing of 4-aminobenzonitriles and 4-amino-3,5-dimethylbenzonitriles at various temperatures​
    Heine, A.; Herbst-Irmer, R.; Stalke, D.; Kühnle, W. & Zachariasse, K. A.​ (1994) 
    Acta Crystallographica / B, 50(3) pp. 363​-373​.​ DOI: https://doi.org/10.1107/S0108768193008523 
    ​Details  DOI 
  • 1993 | Journal Article | 
    ​ ​[Cu2R2BrLi(thf)3], R = Si(SiMe3)3–a complex containing five-coordinate silicon in a three-centre two-electron bond (thf = tetrahydrofuran)​
    Heine, A.; Herbst-Irmer, R.   & Stalke, D. ​ (1993) 
    Journal of the Chemical Society. Chemical communications,(23) pp. 1927​-1731​.​ DOI: https://doi.org/10.1039/C39930001729 
    ​Details  DOI 
  • 1993 | Journal Article | 
    ​ ​A model intermediate for the nucleophilic substitution of (Cp)2Sn; synthesis and structure of (Cp)(Me3Si)2NSn(µ-Cp)Li·pmdeta [Cp = C5H5, pmdeta =(Me2NCH2CH2)2NMe]​
    Paver, M. A.; Russell, C. A.; Stalke, D.   & Wright, D. S.​ (1993) 
    Journal of the Chemical Society. Chemical communications,(17) pp. 1349​-1351​.​ DOI: https://doi.org/10.1039/C39930001349 
    ​Details  DOI 
  • 1993 | Journal Article | 
    ​ ​Two triorganostannate complexes synthesised from bis(cyclopentadienyl)tin(II); structural variation between [Mg(thf)6]2+2[Sn(3-C5H5)3]– and [Li(thf)4]+[Sn(C13H9)3]–(thf = tetrahydrofuran, C13H9= fluorenyl)​
    Edwards, A. J.; Paver, M. A.; Raithby, P. R.; Russell, C. A.; Stalke, D. ; Steiner, A. & Wright, D. S.​ (1993) 
    Dalton Transactions,(9) pp. 1465​-1466​.​ DOI: https://doi.org/10.1039/DT9930001465 
    ​Details  DOI 
  • 1993 | Journal Article | 
    ​ ​Structure of bis(pentamethyldiethylenetriamine)disodium hexasulfide​
    Besser, S.; Herbst-Irmer, R.; Stalke, D.; Wright, D. S.; Snaith, R. & Brooker, A. T.​ (1993) 
    Acta Crystallographica / C, 49(8) pp. 1482​-1483​.​ DOI: https://doi.org/10.1107/S0108270193001167 
    ​Details  DOI 
  • 1993 | Journal Article | 
    ​ ​Lithium- and dimethylaluminium-di-2-pyridyl-phosphides: the first metal diorganophosphides without a metal–phosphorus bond within a contact ion pair​
    Steiner, A. & Stalke, D. ​ (1993) 
    Journal of the Chemical Society. Chemical communications,(5) pp. 444​-446​.​ DOI: https://doi.org/10.1039/C39930000444 
    ​Details  DOI 
  • 1993 | Journal Article | 
    ​ ​Crystal handling at low temperatures​
    Kottke, T. & Stalke, D.​ (1993) 
    Journal of Applied Crystallography, 26(4) pp. 615​-619​.​ DOI: https://doi.org/10.1107/S0021889893002018 
    ​Details  DOI 
  • 1993 | Journal Article | 
    ​ ​Metallation of the acyclic phosphazene ligand HN[P(NMe2)2NSiMe3]2. Synthesis and crystal structure of {NaN[P(NMe2)2NSiMe3]2}2, {KN[P(NMe2)2NSiMe3]2} and Ca{N[P(NMe2)2NSiMe3]2}2​
    Hasselbring, R.; Pandey, S. K.; Roesky, H. W. ; Stalke, D.   & Steiner, A.​ (1993) 
    Dalton Transactions,(22) pp. 3447​-3451​.​ DOI: https://doi.org/10.1039/DT9930003447 
    ​Details  DOI 
  • 1993 | Journal Article | 
    ​ ​Synthesis and structural characterization of diene and benzene pentaruthenium clusters​
    Braga, D.; Grepioni, F.; Sabatino, P.; Dyson, P. J.; Johnson, B. F. G.; Lewis, J. & Bailey, P. J. et al.​ (1993) 
    Dalton Transactions,(6) pp. 985​-992​.​ DOI: https://doi.org/10.1039/DT9930000985 
    ​Details  DOI 
  • 1993 | Journal Article | 
    ​ ​Iminoaminosulfinates: synthesis, crystal structures, and rearrangement monitored by lithium-7 solid-state nuclear magnetic resonance spectroscopy​
    Freitag, S.; Kolodziejski, W.; Pauer, F. & Stalke, D. ​ (1993) 
    Dalton Transactions,(23) pp. 3479​-3488​.​ DOI: https://doi.org/10.1039/DT9930003479 
    ​Details  DOI 
  • 1993 | Journal Article | 
    ​ ​Synthesis and x-ray structure of an isomeric cyclophosphazene complex containing antimony(III)​
    Pandey, S. K.; Hasselbring, R.; Steiner, A.; Stalke, D. & Roesky, H. W.​ (1993) 
    Polyhedron, 12(24) pp. 2941​-2945​.​ DOI: https://doi.org/10.1016/S0277-5387(00)80043-1 
    ​Details  DOI 
  • 1993 | Journal Article | 
    ​ ​A thiouracil-Ca2+ complex containing two tautomeric forms of the thiouracilyl anion: Synthesis and crystal structure of [(thiouracilyl)2Ca·2DMSO·H2O]2​
    Banbury, F. A.; Davidson, M. G.; Edwards, A. J.; Lopez Solera, M.-I.; Raithby, P. R.; Snaith, R. & Stalke, D. et al.​ (1993) 
    Inorganica Chimica Acta, 203(1) pp. 93​-95​.​ DOI: https://doi.org/10.1016/S0020-1693(00)82910-2 
    ​Details  DOI 
  • 1993 | Journal Article | 
    ​ ​Sodium tri(pyrazol-1-yl)-germanate and -stannate: new tridentate claw-ligands containing group 14 metals​
    Steiner, A. & Stalke, D. ​ (1993) 
    Journal of the Chemical Society. Chemical communications,(22) pp. 1702​-1704​.​ DOI: https://doi.org/10.1039/C39930001702 
    ​Details  DOI 
  • 1993 | Journal Article | 
    ​ ​Strukturuntersuchungen an den Produkten aus der Reaktion des Tris(trimethylsilyl)silyllithiums mit Aceton​
    Oehme, H.; Wustrack, R.; Heine, A.; Sheldrick, G. M. & Stalke, D.​ (1993) 
    Journal of Organometallic Chemistry, 452 pp. 33​-39​.​ DOI: https://doi.org/10.1016/0022-328X(93)83169-V 
    ​Details  DOI 
  • 1992 | Journal Article | 
    ​ ​The observation of a Pb–Li bond; synthesis, structure and model molecular orbital (MO) calculations on the monomeric Ph3Pb–Li·(pmdeta) complex [pmdeta =(Me2NCH2CH2)2NMe]​
    Armstrong, D. R.; Davidson, M. G.; Moncrieff, D.; Stalke, D.   & Wright, D. S.​ (1992) 
    Journal of the Chemical Society. Chemical communications,(19) pp. 1413​-1415​.​ DOI: https://doi.org/10.1039/C39920001413 
    ​Details  DOI 
  • 1992 | Journal Article | 
    ​ ​Struktur von [CPRu(C0)2]2 (Cp = η5-pentamethylcyclopentadienyl)​
    Steiner, A.; Gornitzka, H.; Stalke, D. & Edelmann, F. T.​ (1992) 
    Journal of Organometallic Chemistry, 431(1) pp. C21​-C25​.​ DOI: https://doi.org/10.1016/0022-328X(92)83295-S 
    ​Details  DOI 
  • 1992 | Journal Article | 
    ​ ​Ferrocenliganden in der lanthanid-chemie: Chelatstabilisierung des ersten diorganyllanthanid(III)-halogenids​
    Gornitzka, H.; Steiner, A.; Stalke, D.; Kilimann, U.; Edelmann, F. T.; Jacob, K. & Thiele, K.-H.​ (1992) 
    Journal of Organometallic Chemistry, 439(1) pp. C6​-C10​.​ DOI: https://doi.org/10.1016/0022-328X(92)80059-7 
    ​Details  DOI 
  • 1992 | Journal Article | 
    ​ ​Solid-state and solution structures of three lithiumsulfinimidamides: Identification of two distinct structural types​
    Edelmann, F. T.; Knösel, F.; Pauer, F.; Stalke, D. & Bauer, W.​ (1992) 
    Journal of Organometallic Chemistry, 438(1/2) pp. 1​-10​.​ DOI: https://doi.org/10.1016/0022-328X(92)88001-Y 
    ​Details  DOI 
  • 1992 | Journal Article | 
    ​ ​Isolation, structure and MO calculational investigations of a highly stable, hydrogen-bonded primary amine–phosphine oxide adduct, 2-aminobenzothiazole–HMPA, C6H4SC(N)NH2OP(NMe2)3; a possible model to explain the carcinogenicity of HMPA (HMPA = hexamethylphosphoramide)​
    Armstrong, D. R.; Bennett, S.; Davidson, M. G.; Snaith, R.; Stalke, D.   & Wright, D. S.​ (1992) 
    Journal of the Chemical Society. Chemical communications,(3) pp. 262​-264​.​ DOI: https://doi.org/10.1039/C39920000262 
    ​Details  DOI 
  • 1992 | Journal Article | 
    ​ ​Dimere Alkalimetallbenzamidinate: Einfluß des Metallions auf die Struktur​
    Stalke, D.; Wedler, M. & Edelmann, F. T.​ (1992) 
    Journal of Organometallic Chemistry, 431(1) pp. C15​-C5​.​ DOI: https://doi.org/10.1016/0022-328X(92)83291-O 
    ​Details  DOI 
  • 1992 | Journal Article | 
    ​ ​Lithiation and dethiacarbonylation of a heterocyclic thioamide C6H4O·C(S)NH by reaction with solid Li2S in the presence of hexamethylphosphoramide: synthesis and crystal structure of [C6H4O·C(S)NLi·HMPA]2·C6H4(OH)NH2​
    Armstrong, D. R.; Banbury, F. A.; Davidson, M. G.; Raithby, P. R. & Stalke, D. ​ (1992) 
    Journal of the Chemical Society. Chemical communications,(20) pp. 1492​-1494​.​ DOI: https://doi.org/10.1039/C39920001492 
    ​Details  DOI 
  • 1991 | Journal Article | 
    ​ ​Monomere Organosamarium(III) Chalkogenolate durch reduktive Spaltung von E–E-Bindungen (E = S, Se, Te)​
    Recknagel, A.; Noltemeyer, M.; Stalke, D.; Pieper, U.; Schmidt, H.-G. & Edelmann, F. T.​ (1991) 
    Journal of Organometallic Chemistry, 411(3) pp. 347​-356​.​ DOI: https://doi.org/10.1016/0022-328X(91)83040-B 
    ​Details  DOI 
  • 1991 | Journal Article | 
    ​ ​Alkoxysilylamide des Neodyms, Samariums und Ytterbiums: Viergliedrige anorganische Ringsysteme in der Lanthanidchemie​
    Recknagel, A.; Steiner, A.; Brooker, S.; Stalke, D. & Edelmann, F. T.​ (1991) 
    Journal of Organometallic Chemistry, 415(3) pp. 315​-326​.​ DOI: https://doi.org/10.1016/0022-328X(91)80131-3 
    ​Details  DOI 
  • 1991 | Journal Article | 
    ​ ​Four- and eight-membered cyclic phosphazene derivatives of zirconium, titanium and vanadium. Crystal structures of the complexes [ZrCl3(Me3SiNPPh2NSiMe3)]·MeCN and [{TiCl2(OPPh2N)}2]·4MeCN​
    Witt, M.; Stalke, D. ; Henkel, T.; Roesky, H. W.   & Sheldrick, G. M. ​ (1991) 
    Dalton Transactions, pp. 663​.​ DOI: https://doi.org/10.1039/DT9910000663 
    ​Details  DOI 
  • 1991 | Journal Article | 
    ​ ​Synthesis and crystal structure of bis(12-crown-4)lithium bis[N,N-bis(trimethylsilyl)benzenesulphinamidino]lithiate(1–-); the first observation of three different lithium-7 environments in high-resolution solid-state NMR spectroscopy​
    Pauer, F.; Rocha, J. & Stalke, D. ​ (1991) 
    Journal of the Chemical Society. Chemical communications,(20) pp. 1477​-1479​.​ DOI: https://doi.org/10.1039/C39910001477 
    ​Details  DOI 
  • 1991 | Journal Article | 
    ​ ​Lithium-bis(di-tert-butylfluorsilyl)phosphid-ein cyclisches Zwitterion​
    Klingebiel, U.; Meyer, M.; Pieper, U. & Stalke, D.​ (1991) 
    Journal of Organometallic Chemistry, 408(1) pp. 19​-25​.​ DOI: https://doi.org/10.1016/0022-328X(91)80097-4 
    ​Details  DOI 
  • 1991 | Journal Article | 
    ​ ​The preparation and crystal structures of sodium and potassium pentamethylcyclopentadienyl pyridine solvates​
    Rabe, G.; Roesky, H. W.; Stalke, D.; Pauer, F. & Sheldrick, G. M.​ (1991) 
    Journal of Organometallic Chemistry, 403(1/2) pp. 11​-19​.​ DOI: https://doi.org/10.1016/0022-328X(91)83082-F 
    ​Details  DOI 
  • 1991 | Journal Article | 
    ​ ​Comparison of the X-ray crystal structures of the sodium and potassium 2,4,6-tris(trifluoromethyl)phenoxides (RO–) and 2,4,6-tris(trifluoromethyl)benzenethiolates (RS–); [Na(OR)(thf)2]2, [K(OR)(thf)2(µ-thf)]2, [Na(SR)(thf)2·0.25thf]x and [K(SR)(thf)]x(thf = tetrahydrofuran)​
    Brooker, S.; Edelmann, F. T. ; Kottke, T.; Roesky, T.; Sheldrick, G. M. ; Stalke, D.   & Whitmire, K. H.​ (1991) 
    Journal of the Chemical Society. Chemical communications,(3) pp. 144​-146​.​ DOI: https://doi.org/10.1039/C39910000144 
    ​Details  DOI 
  • 1991 | Journal Article | 
    ​ ​Alkali metal derivatives of sulfinimidamides. Preparation and crystal structures​
    Pauer, F. & Stalke, D.​ (1991) 
    Journal of Organometallic Chemistry, 418(2) pp. 127​-145​.​ DOI: https://doi.org/10.1016/0022-328X(91)86360-3 
    ​Details  DOI 
  • 1991 | Journal Article | 
    ​ ​Structure of (Rf)2(Cl)SnIV(μ2-O)SnIV(Cl)(Rf)2; Rf = 2,4,6-tris(trifluoromethyl)phenyl​
    Brooker, S.; Edelmann, F. T. & Stalke, D.​ (1991) 
    Acta Crystallographica / C, 47(12) pp. 2527​-2529​.​ DOI: https://doi.org/10.1107/S0108270191006352 
    ​Details  DOI 
  • 1991 | Journal Article | 
    ​ ​Synthesis and X-ray crystal structure of germaimines​
    Meller, A.; Ossig, G.; Maringgele, W.; Stalke, D. ; Herbst-Irmer, R. ; Freitag, S. & Sheldrick, G. M. ​ (1991) 
    Journal of the Chemical Society. Chemical communications,(16) pp. 1123​-1124​.​ DOI: https://doi.org/10.1039/C39910001123 
    ​Details  DOI 
  • 1991 | Journal Article | 
    ​ ​Diiminophosphinate des Lithiums, Samariums und Ytterbiums: Molekülstrukturen von Li[Ph2P(NSiMe3)2](THF)2 und [Ph2P(NSiMe3)2]2Sm(μ-I)2Li(THF)2​
    Recknagel, A.; Steiner, A.; Noltemeyer, M.; Brooker, S.; Stalke, D. & Edelmann, F. T.​ (1991) 
    Journal of Organometallic Chemistry, 414(3) pp. 217​-335​.​ DOI: https://doi.org/10.1016/0022-328X(91)86331-J 
    ​Details  DOI 
  • 1990 | Journal Article | 
    ​ ​Synthesis and X-ray crystal structure of a tricyclic lead–nitrogen–boron heterocycle​
    Heine, A.; Fest, D.; Stalke, D. ; Habben, C. D.; Meller, A. & Sheldrick, G. M. ​ (1990) 
    Journal of the Chemical Society. Chemical communications,(10) pp. 742​-743​.​ DOI: https://doi.org/10.1039/C39900000742 
    ​Details  DOI 
  • 1990 | Journal Article | 
    ​ ​2,5-Dihydroborole und 1,3-dihydro-1,3-diborete aus 1,3-dienen und aus alkinen durch umsetzung mit dichlor(diisopropylamino)boran und alkalimetallen​
    Bromm, D.; Stalke, D.; Heine, A.; Meller, A. & Sheldrick, G. M.​ (1990) 
    Journal of Organometallic Chemistry, 386(1) pp. 1​-7​.​ DOI: https://doi.org/10.1016/0022-328X(90)80251-T 
    ​Details  DOI 
  • 1990 | Journal Article | 
    ​ ​Spectroscopic and structural characterization of 2,4,6-tris(trifluoromethyl)phenyllithium·Et2O: a dimer stabilized by lithium fluorine contacts​
    Stalke, D.   & Whitmire, K. H.​ (1990) 
    Journal of the Chemical Society. Chemical communications,(11) pp. 833​-834​.​ DOI: https://doi.org/10.1039/C39900000833 
    ​Details  DOI 
  • 1990 | Journal Article | 
    ​ ​Lithiiertes Di-t- butylfluorsilylmesitylphosphan - vom Phosphan zum Phosphid​
    Andrianarison, M.; Stalke, D. & Klingebiel, U.​ (1990) 
    Journal of Organometallic Chemistry, 381(2) pp. C38​-C42​.​ DOI: https://doi.org/10.1016/0022-328X(90)80123-H 
    ​Details  DOI 
  • 1990 | Journal Article | 
    ​ ​1,4,6-Tris(di-isopropylamino)-1,4,6-triboraspiro[4.4]nona-2,8-diene from the reaction of benzene with subvalent boron species​
    Meller, A.; Bromm, D.; Maringgele, W.; Heine, A.; Stalke, D.   & Sheldrick, G. M. ​ (1990) 
    Journal of the Chemical Society. Chemical communications,(10) pp. 741​-742​.​ DOI: https://doi.org/10.1039/C39900000741 
    ​Details  DOI 

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